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(e)-3-[2h-1,3-benzodioxol -5-yl)-1-(7-hydroxy-5-methoxy-2,2-dimethylchroman-8-yl)prop-2-en-1-one

Farediah, Ahmad and Hashim, Nur Athirah and Basar, Norazah and Awang, Khalijah and Seik, Weng Ng. (2011) (e)-3-[2h-1,3-benzodioxol -5-yl)-1-(7-hydroxy-5-methoxy-2,2-dimethylchroman-8-yl)prop-2-en-1-one. Acta Crystallographica Section E-Structure Reports Online, 67 (Pt9). O2301-U2336. ISSN 1600-5368

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Official URL: http://dx.doi.org/10.1107/S1600536811031321


The reaction of 5,6-(2,2-dimethyl­chromane)-2-hy­droxy-4-meth­oxy­acetophenone and 3,4-methlene­dioxy­benzaldehyde affords the title chalcone derivative, C22H22O6. The two benzene rings are connected through a —C(=O)—CH=CH— (propenone) unit, which is in an E conformation; the ring with the hy­droxy substitutent is aligned at 6.2 (1)° with respect to this unit, whereas the ring with the methyl­enedi­oxy substituent is aligned at 8.2 (1)°. The dihdral angle between the rings is 14.32 (7)°. The hy­droxy group engages in an intra­molecular hydrogen bond with the carbonyl O atom of the propenone unit, generating an S(5) ring.

Item Type:Article
Uncontrolled Keywords:benzodioxol, dimethylchroman
Subjects:R Medicine > RA Public aspects of medicine
ID Code:44672
Deposited By: Haliza Zainal
Deposited On:21 Apr 2015 03:31
Last Modified:31 Jan 2017 06:46

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